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In the case of the intermolecular isotope effect, the decarboxylation of benzoic acid 7 14C can be cited as an example Here, one is usually dealing with the dec2 2 arboxylation of two compounds: C6 H52 14 COOH and C6 H52 12 COOH Again, 2 since the 12 C2 14 C bond is relatively more stable, we would expect that during the initial phase of the decarboxylation reaction there would be an enrichment of 12 CO2 compared to the speci c activity of the labeled carbon in the benzoic acid As the reaction approaches completion, however, the reactant (benzoic acid) will be relatively enriched with the 14 C-labeled variety, and, consequently, the decarboxylation product (CO2) will have a speci c activity higher than the labeled carbon of the original starting material.

When the reaction is driven to completion, the overall speci c activity of CO2 will naturally be the same as the labeled carbon atom in the benzoic acid; that is, no isotope effect can be observed This is an important concept for it indicates that the signi cance of the isotope effect can be minimized or ignored in radiotracer studies if the intramolecular type of reaction is not involved The second basic assumption is that the radioactivity does not change the chemical and physical properties of the experimental system It is essential that the radiation dose from the tracer does not elicit a response from the experimental system that would distort the experimental results The amount of activity employed should be restricted to the minimum necessary to permit reasonable counting rates in the samples to be assayed.

{dn}

23 I23

The possibility of excessive concentration of the tracer compound in certain biological tissues and the degree of radiosensitivity of these tissues must also be carefully considered, especially when a- or b2-emitting tracers are used Fortunately, the excellent sensitivity of most radioactivity assay methods minimizes the need to employ tracer doses of such a magnitude that any detectable radiation damage occurs The possibilities of interference due to physiological response to radiation are further minimized because most studies are short term and thus completed before any latent radiation effects appear In physical tracer studies, the radiation damage produced by the decaying nuclei must not so destroy the crystal structure and similar features as to modify the experimental results In addition, one must remember that as the result of radioactive decay, the daughter atom is usually a different chemical element than the mother atom.

12.16 12.17

One must be sure that the presence of these foreign species and any related equilibria does not affect the observations (For example, if both the mother and daughter atoms are b2 emitters, then one might see a increase in the count rate due to the inability to distinguish the b2 particles from the tracer and its daughter).

1 To create the list box, double-click the grid that contains the artwork for the audio player to make it the active container Then click the ListBox button in the Toolbox, and click and drag in the grid to create the list box there You can use the Layout palette to finetune the list box s size and location Then right-click on the list box and choose Add ListBoxItem Do this for as many files as you want in your audio player 2 To add the audio files into the project, choose Project Add Existing Item, navigate to your files, select them, and click Open The files appear in the Files palette of the Project panel 3 Double-click the audio player to make it active 4 Click the Create New Timeline button in the Objects and Timeline palette.

This chapter provides a comprehensive overview of reactive absorption and discusses in detail the following issues: important industrial applications reactive absorption equipment modeling basics and different modeling concepts model parameter estimation four different industrial case studies, namely NOx absorption coke gas purification CO2 absorption by amines SO2 absorption into aqueous NaHCO3/Na2CO3 solutions

To use a function in your script, specify the function name on a line, just as you would any other shell command:

Name the timeline the name of one of your audio files (without the extension) and click OK Rightclick on the name of the audio file in the Files palette, and in the pop-up menu that appears click Insert Then click the Record Mode button to off 5 Repeat step 4 for each audio file that you want to add 6 Then name your list box items with the names of your audio files in the Name property at the top of the Properties panel Type in the name of each song (or audio file) without spaces and capitalize first letters for readability And select the list box item, right-click on it, and in the pop-up menu that appears choose Edit Text Then type in the name Spaces are okay here 7.